Applies to: Chromatography Smart (GC/MS) Tickets Solved: 0 Rank: 8.8
A concentrator can break in two distinct ways. One is a visible break which can be seen through inspection of the concentrator. If a break is visible the following steps should be taken:
The second possibility is that the concentrator has a hairline fracture in the glass tube. This fracture is often invisible to the naked eye. The best way to isolate this deficiency is to try to complete the concentrator method with a new concentrator installed.
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Keywords: concentrator, debris, column pressure, "dirty runs", sample loop